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Ep2298720b1 ep10184100.5a ep10184100a ep2298720b1 ep 2298720 b1 ep2298720 b1 ep 2298720b1 ep 10184100 a ep10184100 a ep 10184100a ep 2298720 b1 ep2298720 b1 ep 2298720b1 authority ep european patent office prior art keywords glycerol catalyst reaction acetol propylene glycol prior art date legal status the legal status is an assumption and is not.
Susmita das, vimal chandra srivastava, synthesis and characterization of copper succinate and copper oxide nanoparticles by electrochemical treatment optimization by taguchi robust analysis, the canadian journal of chemical engineering, 10.22478, 94, 7, 1322-1327, 2016.
The invention claimed is 1.A process for preparing acrolein by dehydrating glycerol in the presence of a solid-state catalyst which comprises at least one tungsten compound selected from the group consisting of ammonium tungstate, tungstic acid, and tungsten oxides and has a hammett acidity h o of 2 and which includes at least one promoter compound selected from the group consisting of.
Highly dispersed copper nanoparticles supported on silica were successfully prepared by a simple and convenient precipitationgel technique, and their physicochemical properties and activity were compared to those of a catalyst prepared by the conventional impregnation method.As a consequence of the preparation method, the texture bet, dispersion dissociative n2o adsorption, morphology.
Glycerol carbonylation with urea is a very feasible option to produce glycerol carbonate with a net result of co2 fixation through urea synthesis.The prerequisite of an efficient catalyst for this reaction is to possess both acid and basic sites together.Several acidic supports were screened for zno catalyst in this work and znmcm-41 was found to exhibit the best activity and almost.
Preparation of silver powder through glycerol process ethylene gl ycol 197 3c and hence it facilitates a high er reaction temper ature though silver powder has been pre pared through polyol route using ethylene glycol and pvp as reducing agents the use of glycerol to prepare silver powder has not been studied in the present inve stigation.
A novel process was developed to produce spherical copper powder for multilayer ceramic capacitors mlcc.Spherical ultrafine cuprous oxide cu2o powder was prepared by glucose reduction of cuoh2.The cu2o particles were coated by mgoh2 and reduced to metallic copper particles.At last, the copper particles were densified by high-temperature heat treatment.
Hydrogenoil ratio, glycerol concentration, and alkaline additives on the catalytic performance were also studied.2 experimental 2.1 catalyst preparation the supported raney-cual 2 o3 was prepared by the fol-lowing processes copper-aluminum alloy powder with a mass ratio of cual4852, and a particle size of150 m.
A high surface area mesoporous tio 2 material 110 m 2 g was synthesised using a nanocasting methodology, utilizing sba15 as a hard template.This material was subsequently used as a support to prepare a series of 1 wt.Aupttio 2 catalysts, synthesised by conventional impregnation and solimmobilisation.Catalysts were tested for the oxidation of glycerol to lactic acid and their.
The preparation of metal nanostructures has received much attention because of their potential applications in the fields of information storage,.The x-ray powder diffraction.These images show the evolution process of the copper nanostructures developing into the final observed nanocubes during a typical synthesis process.
Cosmetic or dermatological powder, its preparation process and its uses.United states patent 5607666.Abstract powders that have been obtained from a homogenized and dehydrated oil-in-water emulsion containing a a structuring and emulsifying agent, b at least one fat, c at least one cosmetically active substance, and d an aqueous.
The hydrogenolysis of glycerol is a multifaceted process in which acid sites and metal sites of the catalyst are indeed the crucial elements for the selective formation of 1,2-pdo and 1,3-pdo.
Because of distinctive properties, such as dendritic structure, high green strength, and low oxygen content, electrolytic copper powder has been widely used in aviation, aerospace, national defense industry and other domains.But at present, energy consumption of the electrolysis process in copper powder production is high, and the current efficiency is only about 90.
Powder coating copper busbar coating systems inc.The powder coating process may seem like it shouldnt work because we are coating a surface with a dry epoxy rather than a wet paintlike material powder coatings stay in place not because they dry and adhere to the copper busbar but because we give the epoxy or the ectfe powder an electrostatic charge that allows the two surfaces to bond on a.
The synthesis of copper nanoparticles cu nps stable to chemical oxidation has attracted much attention due to their novel application possibilities.The physicochemical properties of cu nps define their utilization in diverse fields, including biological applications, solar cells, high conductivity inks for printed electronics, and other specific applications.
Due to oxidizability of copper coating on carbon nanotubes, the interfacial bond strength between copper coating and its matrix is weak, which leads to the reduction of the macroscopic properties of copper matrix composite.The electroless coating technics was applied to prepare nickel-copper bilayers coated on single-walled carbon nanotubes.
Borikar et al prepared copper 10, nickel 11, cadmium 12 and zinc 13 powders by electrowinning process, in acetone and sulphuric acid medium.Viswanath and george reported preparation of electrolytic nickel powder 14 by electrowinning process from glycerol.
In recent years, the rapid swift increase in world biodiesel production has caused an oversupply of its by-product, glycerol.Therefore, extensive research is done worldwide to convert glycerol into numerous high added-value chemicals i., glyceric acid, 1,2-propanediol, acrolein, glycerol carbonate, dihydroxyacetone, etc.Hydroxyl acids, glycolic acid and lactic acid, which comprise of.
Preparation of copper powder by glycerol process | amit.A simple, least energy intensive, efficient, low temperature chemical process for the production of copper powder of narrow size distribution is described.Service online us7682581b2 - method for the removal of copper from a zinc.
Preparation of dispersive nanocrystalline copper powders by chemical reduction method under ultrasonic condition was investigated using copper sulfate as a raw material,hydrazine as a reductive agent and surfactants as modifiers.The effects of dosage and kind of surfactants on the shapes,sizes and size distributions of nanocrystalline copper powders were investigated.The ultrasonic effect was.
Production of glycerol carbonate i comprises reacting glycerol with urea at 90-220 degrees c in the presence of a catalyst having lewis acid sites associated with heteroatom anionic counter ions i.Not carbonate ions.Ep0955298a1 - process for the preparation of glycerol carbonate - google patents process for the preparation of glycerol.